Preparation and condensation reactions of a new light-fluorous Mukaiyama reagent: reliable purification with fluorous solid phase extraction for esters and amides

Masato Matsugi,Masakazu Hasegawa,Daisuke Sadachika,Sachina Okamoto,Mami Tomioka,Yoshimi Ikeya,Araki Masuyama,Yuji Mori

doi:10.1016/j.tetlet.2007.03.173

Preparation and condensation reactions of a new light-fluorous Mukaiyama reagent: reliable purification with fluorous solid phase extraction for esters and amides

Masato Matsugi, Masakazu Hasegawa + Show 6 more

https://doi.org/10.1016/j.tetlet.2007.03.173

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Journal: Tetrahedron Letters	Publication Date: Apr 6, 2007
Citations: 23

Affiliation: Meijo University, Osaka Institute of Technology

#Fluorous Solid Phase Extraction #Fluorous Phase + Show 8 more

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Abstract

A modified light-fluorous Mukaiyama reagent bearing a C 8F 17 tag was prepared and examined in ester and amide forming condensation reactions. Following the reactions, the desired product was effectively separated from the fluorous pyridone by-product using a simple fluorous solid phase extraction.

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