Abstract
A titanosilicate with the crystal structure of zeolite ZSM-5 was prepared via the non-alkaline “fluoride” route using rutile as the source of titanium. The properties of the product are compared with those of silicalite, the purely siliceous analogue of ZSM-5, and a sample prepared by a post-synthesis treatment of silicalite with TiCl 4. Zeolites [Si,Ti]-ZSM-5 selectively catalyse the liquid-phase oxidation of cyclohexanol to cyclohexanone.
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