Abstract
4-Vinylbenzoic acid reacted with Ru 2(D(3,5-Cl 2Ph)F) 3(OAc)Cl and cis-Ru 2(D(3,5-Cl 2Ph)F) 2(OAc) 2Cl (D(3,5-Cl 2Ph)F is N, N′ -bis(3,5-dichlorophenyl)formamidinate) to yield Ru 2(D(3,5-Cl 2Ph)F) 3(4-vinylbenzoate)Cl ( 1) and cis-Ru 2(D(3,5-Cl 2Ph)F) 2(4-vinylbenzoate) 2Cl ( 2), respectively. Ru 2(D(3,5-Cl 2Ph)F) 3(OAc)Cl reacted with 5-hexenoic acid and 6-heptenoic acid to afford Ru 2(D(3,5-Cl 2Ph)F) 3(5-hexenoate)Cl ( 3) and Ru 2(D(3,5-Cl 2Ph)F) 3(6-heptenoate)Cl ( 4), respectively. All new compounds were characterized using voltammetric and Vis–NIR spectroscopic techniques, and the structures of 1 and 2 were also established through X-ray single crystal diffractions.
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