Abstract
A procedure for the determination of oxygen in ceramic oxide superconductor samples of the La/Sr/Cu/O type is described. The method relies upon the precise measurement of the metallic element concentrations by flame spectrometry. Oxygen content is subsequently determined by titrimetry using a bromometric technique. A calculation algorithm, based on principles of charge and mass balances, was employed to estimate values for the stoichiometric coefficients in superconducting ceramic samples. Results emphasize the importance of previous chemical analysis accuracy on the determination of oxygen content.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
