Abstract

The activation energy of the β → α/ω phase transformation increased monotonously with the application of a continuous heating process to a Ti-15Mo-2.7Nb-3Al-0.2Si alloy. Precipitation behaviour of the alloy aged at different temperatures were analysed with scanning electron microscopy, electron backscattered diffraction and transmission electron microscopy. Selected-area diffraction patterns of the ω, ω/α and α phases in the alloy aged at different temperatures indicated that the type of phase transformation was influenced by the precipitation process. Precipitate-free zones in the alloy aged at 450 °C for 8 h were harmful to the mechanical performance. Fine α precipitates with an obvious texture were obtained in the alloy aged at 500 °C. A good combination of tensile properties with an ultimate tensile strength of 1310 MPa and an elongation of 13.5% were obtained due to the expected microstructure and texture of the precipitates that transformed in the specimen when it was aged at 500 °C for 8 h. The size of the precipitates increased with increasing aging temperature. Furthermore, the amount of precipitates and their degree of texture decreased substantially in the alloy aged at 600 °C. The investigation of the tensile properties and fractures also revealed a correlation between the mechanical properties and precipitation behaviour in the Ti-15Mo-2.7Nb-3Al-0.2Si alloy aged at different temperatures.

Highlights

  • The evolution of the microstructure and its effect on the performance of beta titanium alloys has been reported in the literature[10,11,12,13,14,15,16]

  • The value of the activation energy for phase transformation can be obtained from the results of the endothermic peaks in the differential scanning calorimeter (DSC) measurements performed with different heating rates

  • The microstructure and tensile properties in the alloy aged at different temperatures were investigated by scanning electron microscopy (SEM), electron back scattered diffraction (EBSD), transmission electron microscopy (TEM) and tension testing

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Summary

Introduction

The evolution of the microstructure and its effect on the performance of beta titanium alloys has been reported in the literature[10,11,12,13,14,15,16]. Nag et al.[19] reported that refined α precipitates transformed in the β matrix of Ti-15Mo and TMZF biomedical alloys during 600 °C aging. The alloy was designed as an alternate material for Ti-6Al-4V to solve the requirements of high strength fasteners in the aerospace industry. This alloy would be optimized to achieve excellent mechanical performance after solution and aging treatments. Tensile properties and fractures of the alloy were studied to reveal the correlation between the mechanical properties and precipitate behaviour in the alloy aged at different temperatures

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