Abstract
A new chemical preparation of silver iodate AgIO 3 is given. The crystal structure has been determined by single-crystal X-ray diffraction methods and refined to a final R value of 0.051 for 1280 independent reflections. The unit cell is orthorhombic with a = 7.265(2), b = 15.17(4), c = 5.786(2)A˚, Z = 8. The space group is Pbc2 1. IO 3 groups and AgO 6 octaedra form a compact bidimensional framework perpendicular to the b axis.
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