Practical method to determine the effective zero-point of indentation depth for continuous stiffness measurement nanoindentation test with Berkovich tip

Abstract

The zero-point of indentation depth in nanoindentation or depth-sensing instrumented indentation tests should be precisely set to evaluate the indentation hardness and indentation elastic modulus of materials to be tested, especially at shallow depths. A critical contact stiffness value has been widely used to determine the zero-point in nanoindentation tests with a Berkovich tip using the continuous stiffness measurement (CSM) method. However, this criterion occasionally gives an inadequate zero-point owing to the surface roughness of materials, the vibration of the testing system, and the flaws of the CSM method at shallow depth. This study proposes a practical method to determine the effective zero-point of indentation depth, which was obtained linearly at the zero-point of contact stiffness and extrapolated from the depth-dependent contact stiffness values, except for those at initially unstable contact depths. The proposed method enables nanoindentation tests to obtain a constant indentation elastic modulus and low deviation of nanoindentation hardness of homogenously fused silica and metallic materials, which provides an efficient way to obtain more accurate test data.