Abstract
A second-generation synthesis of synthetic 6-O-methyl-D-glucose-containing polysaccharides (sMGPs) is reported. Glycosidation acceptor A and donor B are prepared from alpha-, beta-, and gamma-cyclodextrins in high yields. The glycosidation of A and B, followed by deprotection, furnishes sMGP 12-, 14-, and 16-mers. This synthesis has appealing features such as scalability, operational simplicity, and high overall yield.
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