Abstract
Potassium iodide-mediated radical sulfonylation/1,2-carbon migration sequences of alkenylcyclobutanols has been developed. The reaction was effectively accelerated using potassium iodide as a catalyst under mild reaction conditions without other metal oxidant. This approach is environmentally benign by use of shelf-stable arylsulfonyl hydrazides as arylsulfonyl radical precursor and water as solvent. This approach offers a facile way to prepare β-sulfonated cyclic ketone derivatives.
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