Abstract
AbstractAn efficient synthesis of methyl heptaglucoside 2 using poly(ethyleneglycol)monomethyl ether as a polymer support is described. Elongation of the acceptor 11, anchored via a succinoyl linkage to PEG, with the appropriate glycosyl donors 4–6 and intermittent protective group manipulations gave fully protected heptamer 18. Deprotection of 18 furnished, after purification as its peracetate, title compound 2 in a good overall yield.
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