Polarization transfer via long range couplingas a simple one-dimensional NMR technique for 1H- 13C correlation. Application to the definitive assignment of the syn and anti 13C δ resonances of 2-substituted adamantanes

Ashraf N Abdel-Sayed,Ludwig Bauer

doi:10.1016/s0040-4039(86)80033-8

Polarization transfer via long range couplingas a simple one-dimensional NMR technique for 1H- 13C correlation. Application to the definitive assignment of the syn and anti 13C δ resonances of 2-substituted adamantanes

Ashraf N Abdel-Sayed, Ludwig Bauer

https://doi.org/10.1016/s0040-4039(86)80033-8

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Journal: Tetrahedron Letters	Publication Date: Jan 1, 1986
Citations: 25

Affiliation: University of Illinois at Chicago

#Syn Protons #Polarization Transfer + Show 8 more

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Abstract

The syn and anti δ resonances in 13C NMR spectra of 2-substituted adamantanes wereassigned unequivocally by means of selective polarization transfer from γ- syn protons via 2-bond carbon-proton coupling.

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