Abstract
Orthorhombic TlBF 4 III transforms at 201.7°C to cubic TlBF 4 II, and at 26.6°C, 6.73 ± 0.60 kbar to a high-pressure phase TlBF 4 IV similar to Bridgman's high-pressure form of TlClO 4. The high-pressure phase diagrams of TlClO 4 and TlBF 4 were studied by means of differential thermal analysis and volumetric techniques, and found to be closely similar to those of RbClO 4 and RbBF 4.
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