Abstract
We have developed a x-ray microprobe in the energy region from 6 to 20 keV using undulator radiation and zone-plate optics for microfocusing-based techniques and applications at a beamline at the Advanced Photon Source (APS). The performance of the beamline was shown to meet our design objectives, including preservation of the source brilliance and coherence, selectable transverse coherence length and energy bandwidth, high angular stability, and harmonic suppression of the beam. These objectives were achieved by careful thermal management and use of a novel mirror and crystal monochromator cooling geometry. All beamline optical components are water cooled, and the x-ray beam in the experiment station is stable in beam intensity, energy, and position over many days with no active feedback. Using a double-crystal Si(111) monochromator, we have obtained a focal spot size (FWHM) of 0.15 μm(v)×1.0 μm(h), and a photon flux of 4×109 photons/sec at the focal spot, and thus a photon flux density gain of 15,000. A circular beam spot of 0.15 μm in diameter can be achieved by reducing the horizontal source size using a white beam slit located 43.5 meters upstream of the zone plate, with an order of magnitude less flux in the focal spot.
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