Abstract
The accuracy of the analytical procedure was checked by the analysis of the standard reference materials: stainless steel (AISI 321) SRM 121-d and highly alloyed steel (Eurostandard 281-1). The precision, expressed as the relative standard deviation, and the detection limits were also reported for each voltammetric technique. The selectivity of the above-mentioned three techniques was found to increase in the following order: second harmonic alternating current adsorption voltammetry > differential pulse adsorption voltammetry > fundamental harmonic alternating current adsorption voltammetry
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