Abstract
AbstractPb2(OH)2[p‐O2C‐C6H4‐CO2]: Synthesis and Crystal StructureSingle crystals of Pb2(OH)2[p‐O2C‐C6H4‐CO2] (1) were obtained by hydrothermal reaction of terephthalic acid and PbCO3 at 180 °C (10 days). 1 crystallizes in the monoclinic space group P21/c with Z = 2 (a = 1115.6(2) pm, b = 380.10(4) pm, c = 1141.3(2) pm, β = 93.39(1)°, V = 0.4831(1) nm3). The crystal structure is characterized by ladder‐type Pb(OH)3/3 double chains, which are connected to a three‐dimensional framework by terephthalate dianions.
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