Abstract
Abstract The rate of ligand exchange in a U(V)-DMF complex was determined for the first time in N,N-dimethylformamide(DMF) at temperatures below −40°C by using the 1H NMR method. The paramagnetic shift by U(V) was also observed in the 1H and 13C NMR signals of bulk DMF owing to the fast exchange between the first coordination sphere of U(V) and the bulk solvent at 25°C.
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