Abstract
Alkenyl-monoalkoxydimethylsilanes, dialkoxymethylsilanes, and trialkoxysilanes undergo palladium-catalyzed cross-coupling reaction with alkenyl and aryl halides in the presence of tetra- n-butylammonium fluoride. A one-pot transformation of a homopropargyl alcohol to regio- and stereo-defined trisubstituted homoallyl alcohols has been achieved by a sequence of intramolecular hydrosilation and the palladium-catalyzed coupling reaction.
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