Abstract
Abstract A Pd-catalyzed dehydrogenative [3+3] aromatization of 3-phenylpropyl ketones and allyl carbonates has been developed. The reaction gives various di- or tri-substituted aromatic ketones. The reaction consisting of five steps efficiently proceeded in a one-batch, one-manipulation setup. The postulated active species, η3-allyl palladium complex, works as a catalyst for triple dehydrogenations and mono allylation with high substrate controls.
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