Abstract
Methods for the synthesis of new palladium(II) acetate complexes [L2Pd(OCOCH3)2], where L is N-coordinated morpholine (C4H9ON) or 4-methylmorpholine (C5H11ON), have been developed. The structure of the complex (C4H9ON)2Pd(OAc)2 · 2H2O (1) has been established by X-ray diffraction. The crystals of 1 are monoclinic (C12H26O8N2Pd, M = 434.76), space group P2(1)/c, a = 9.129(3) A, b = 16.227(5) A, c = 6.159(2) A, V = 878.5(5) A3, Z = 2. The palladium atom has a square-planar environment with the trans arrangement of ligands. The complex (C5H11ON)2Pd(OAc)2 (2) has a similar structure, according to spectroscopic data.
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