Abstract
Mercury EDTA dehydrogenation of 2-(pyrrolidinomethyl)-pyridine-1-oxide ( 1) yields the pyrrolidone 5, which may be accounted for by a neighbouring effect of the amine oxide group. For an additional basic product the structure of ( E)-2-(1-pyrroline-3-ylidenemethyl)-pyridine-1-oxide ( 11) has been proved by X-ray crystallography and synthesis. This indicates a cleavage of the doubly dehydrogenated product followed by recombination.
Published Version
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