Abstract
Exploiting hydrothermal technique, a new cobalt-vanadate termed Co(en)2[VIV4VV2O14] was prepared, where en stands for ethylenediamine. For its elucidation, a combination of powder X-ray diffraction, FT-IR, X-ray single-crystal diffraction and elemental analysis was performed. The compound displays a 3D configuration consisting of mixed -valence vanadium (IV,V) oxide layers and metal–organic bridges. The catalytic potential of compound 1 for the heterogeneous oxidative sulfides is strong, and 1 is reusable without activity depletion. Furthermore, the magnetic behavior demonstrates the antiferromagnetic interactions in 1.
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