Abstract
Unsaturated primary alcohols and ω-haloalkanols, all applied in pheromone synthesis, are oxidized to the corresponding aldehydes using 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxo--ammonium tetrafluoroborate ( 1A). Three methods are compared with one another; oxidations with 1A and silica gel, oxidations with 1A in the presence of pyridine, and pyridinium chlorochromate (PCC).
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