Abstract

Out-of-plane permeability of reinforcement preforms is of crucial importance in the infusion of large and thick composite panels, but so far, there are no standard experimental methods for its determination. In this work, an experimental set-up for the measurement of unsaturated through thickness permeability based on the ultrasonic wave propagation in pulse echo mode is presented. A single ultrasonic transducer, working both as emitter and receiver of ultrasonic waves, was used to monitor the through thickness flow front during a vacuum assisted resin infusion experiment. The set-up was tested on three thick carbon fiber preforms, obtained by stacking thermal bonding of balanced or unidirectional plies either by automated fiber placement either by hand lay-up of unidirectional plies. The ultrasonic data were used to calculate unsaturated out-of-plane permeability using Darcy’s law. The permeability results were compared with saturated out-of-plane permeability, determined by a traditional gravimetric method, and validated by some analytical models. The results demonstrated the feasibility and potential of the proposed set-up for permeability measurements thanks to its noninvasive character and the one-side access.

Highlights

  • The aim of this work is to present a new experimental set-up for the measurement of unsaturated through thickness permeability based on the ultrasonic wave propagation in pulse echo mode, i.e., by using only one ultrasonic transducer working both as emitter and receiver of ultrasonic waves

  • An experimental set-up for the measurement of unsaturated through thickness permeability based on the ultrasonic wave propagation in pulse echo mode was proposed

  • The new measurement method was tested on three thick carbon fiber preforms, obtained by stacking and vacuum bagging or by automated fiber placement of unidirectional plies

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Summary

Introduction

By combining the attractive features of different constituents, composite materials can be properly designed for specific applications, replacing traditional materials in an ever-increasing variety of products and applications in aerospace, automotive, marine, nanocomposite, construction, etc. [1,2,3].More recently, the emerging trend towards lightweight, high performance, high functionality and high sustainability components is driving the research towards nanocomposites, multi-material hybrid structures and composites derived from renewable resources or from reusing approaches [4,5,6,7,8,9].The growing demand of polymer matrix composites in several fields has driven the research and development of new manufacturing processes. The challenge of manufacturing high quality and complex geometry components at relatively low cost and fast cycle times has pushed toward the development of liquid composite molding (LCM) processes [10,11]. These technologies usually involve the use of dry reinforcement preforms, an assembly of dry fiber layers that have been pre-shaped to the form of the desired product and bonded together using a binder resin, which are impregnated by resin injection or infusion into a mold [12,13].

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