Abstract
The synthesis and characterization of four organomercury derivatives of 1-phenyl-3-methyl-4-acyl-5-pyrazolones (L), RHgL (R Me, Ph; acyl = acetyl, benzoyl), are described. The report includes the crystal structure of one compound, PhHg[1-Ph-3-Me-4-PhCO-5-C 2N 2CO], which represents the first crystallographically authenticated mercury β-diketonate bonded to the metal through oxygen, and also the first structural report on an organomercury β-diketonate. For comparison, the two diphenylthallium derivatives of the same two pyrazolone ligands have also been prepared.
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