Abstract
The determination of alkoxyl and alkimino groups has been extended to compounds which produce from methyl to hexyl iodide on treatment with hydriodic acid. An apparatus is described for the decomposition and collection of the alkyl iodides, followed by gas Chromatographic separation and determination on the 0.1 milliequivalent scale. Single compounds and mixtures containing both alkoxyl and alkimino groups have been successfully analyzed.
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