Abstract
The reactions between niobium penta-ethoxide and organic esters ( n-propyl, isopropyl, n-butyl, sec.-butyl, tert.-butyl, n-amyl and phenyl acetate) have been studied using the organic esters also as solvent, except in the cases of n-amyl and phenyl acetates, where cyclohexane was used as a solvent. This technique provides a suitable method for the synthesis of niobium penta- tert.-butoxide.
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