Abstract

Chrom red brown 5RD was used as an indicator for complexometric titration of thorium. The change in the colour at the end-point was from wine-red to yellow. It is recommended that the thorium buffered aliquot should not contain less then 200 μg thorium per 10 ml for a precise estimation. A range of pH from 2.5 to 3.5 has been found satisfactory for such a titration. Ferri, ferro and zirconium ions interfere; they should be separated beforehand.

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