Abstract

Ds-type inclusions during production are an important factor affecting the performance and quality of manufactured 10B21 steel. To minimize Ds-type inclusions in steel and improve the production qualification rate of steelmaking plants, a refining slag system optimization scheme was proposed based on the analysis of current inclusion evolution during the steelmaking process, and industrial tests were conducted to verify improvements resulting from application of the proposed scheme. The results showed that the composition of Ds inclusions in 10B21 steel are mainly CaO–Al2O3–MgO–CaS–TiN, which exists in the form of calcium–magnesium aluminate coated with titanium nitride and calcium sulfide. The main reason for the formation of Ds inclusions is the poor fluidity of the refining slag and its low capability to absorb inclusions. The poor coverage of the refining slag on the molten steel during refining can easily cause secondary oxidation of the molten steel. Thus, the formation and growth of Ds-type inclusions are aggravated after the calcium feeding line and soft blowing operation. Here, we propose to minimize Ds inclusions using our optimized refined slag system. The mass percentage of the optimized slag system is CaO: 55–60%, Al2O3: 20–35%, SiO2: 3–7%, MgO: 4–8%, (MnO + FeO) < 1%, and the basicity is controlled within the range of 7–11. We observed that our optimized refining slag system has a significantly improved ability to remove inclusions, particularly Ds inclusions, which improves the qualification rate of 10B21 steel.

Highlights

  • CaO–Al2 O3 –MgO–CaS–TiN, which existed in the form of calcium–magnesium aluminate coated with titanium nitride and calcium sulfide

  • CaO–Al2O3–MgO–CaS–TiN, which existed in the form of calcium–magnesium aluminate coated with titanium nitride and calcium sulfide

  • The composition of Ds inclusions that affect the quality of 10B21 steel is mainly

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Summary

Introduction

Publisher’s Note: MDPI stays neutral with regard to jurisdictional claims in published maps and institutional affiliations. Cold heading is an important method for forming standard parts such as fasteners and connectors. Numerous studies show that refining slag is an important factor influencing nonmetallic inclusion formation in steel. We sought to control the problem of excessive Ds inclusions in 10B21 steel produced by a specific enterprise, by first analyzing the entire process. From this analysis, it was determined that the formation of Ds inclusions were concentrated in the LF refining step, so a comprehensive analysis of the refining slag system of Ds inclusions was conducted and, based on this, an optimization plan for the refining slag system was proposed. This plan was subject to industrial testing, and the resulting 10B21 rolling material was rated for inclusions, and the results of the inclusion classification are compared to those before optimization and analyzed

Production Process
Sample Preparation and Testing
Evolution of Inclusions during the Steelmaking Process
Analysis of beforeinOptimization
Optimization of the Refining Slag System and Industrial Testing
Refining Slag Content Optimization
CaO–Al22O33–SiO
CaO–Al
Findings
Conclusions
Full Text
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