Optimization study for preparation of activated carbon from Acacia mangium wood using phosphoric acid

Abstract

A study on the preparation of activated carbon from Acacia mangium wood was conducted, and the operating factors, such as activating agent concentration, activation temperature and activation time, were optimized using response surface methodology. In order to determine the effects of the operating factors namely H3PO4 concentration (6.48–48.5 %), activation temperature (364–1,036 °C) and activation time (19–146 min) on the characteristics of activated carbon, a three-level rotatable central composite design was used. The second-order mathematical model was proposed by regression analysis of the experimental data gathered from 20 batch runs. The optimum H3PO4 concentration, activation temperature and activation time were found to be 40 %, 900 °C and 45 min, respectively. At optimum conditions of the operating factors, the percent yield and surface area were 20.3 % and 1,767 m2/g, respectively. The activated carbon was found to be largely composed of mesopores. About 95 % of the total surface area was attributed to mesopores.