Abstract

Statistical analysis of product yield for biodiesel preparation by transesterification process was performed using the Minitab software. A standard RSM Design tool known as CCD was applied to study the transesterification reaction variables. The obtained parameters were verified experimentally for the transesterification reaction of rubber seed oil using solid metal oxide catalyst. The factors affecting the methyl ester yield during transesterification reaction were identified as the catalyst content, molar ratio of oil to alcohol and reaction time. High methyl ester yield and fast reaction rate could be obtained even if reaction temperature was relatively low, which is quite favorable to the industrial production of biodiesel from the rubber seed oil. 98.54% of methyl ester was formed from the transesterification of RSO with methanol. R-squared is a statistical measure of how close the data are to the fitted regression line. It is also known as the coefficient of determination, or the coefficient of multiple determination for multiple regression. In this study, an R2 value of 0.98 is obtained.

Highlights

  • Biodiesel is defined as a fuel comprised of mono-alkyl esters of long chain fatty acids derived from vegetable oils or animal fats

  • The present investigation aims to evaluate the performance of the solid metal oxide catalyst, CaO for the transesterification reaction of rubber seed oil

  • Many researchers recognized that one of the main factors affecting the yield of biodiesel is the molar ratio of alcohol to oil

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Summary

Introduction

Biodiesel is defined as a fuel comprised of mono-alkyl esters of long chain fatty acids derived from vegetable oils or animal fats. It is non-toxic, biodegradable and available, has a high heat value, high oxygen content (10 to 11%) and does not contain sulfurs and aromatic compounds. The current feed stocks for production of biodiesel or mono-alkyl ester are vegetable oil, animal fats and micro algal oil. Experimental studies will be conducted to investigate the effects of main parameters, including methanol to rubber seed oil ratio, catalyst to oil weight ratio, reaction temperature and reaction time to obtain the optimal condition [1]-[4]

Materials & Methods
Biodiesel Preparation
Theoretical Optimization
Central Composite Design
Alcohol to Oil Molar Ratio
Catalyst to Oil Weight Ratio
Optimization of Reaction Temperature
Optimization of the Reaction Time
Conclusion
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