Online thickness measurements of acrylate-based coatings on knitted polyester fabric using terahertz time-domain spectroscopy

Abstract

Three different institutions combined their expertise in a joint R&D project to demonstrate the suitability of terahertz time-domain spectroscopy for thickness measurements of acrylate-based coatings on polyester fabric. First, we spectroscopically analyzed the materials involved using a high-precision terahertz spectrometer and determined optical properties such as the refractive index and loss coefficient. Raster scans were then performed across the sample, and terahertz images were created to identify material boundaries and thickness inhomogeneities. Finally, we applied a fast scanning terahertz time-domain spectrometer based on electronically controlled optical sampling and a customized reflection head for online thickness measurements in a coating line. The textile moved at a speed of 0.5 m/min, while the measurement system records terahertz pulses at a rate of 1600 traces/s. Coating thicknesses of between 63 µm and 99 µm were calculated in a post-processing step. To classify these non-contact and non-destructive measurements, these thicknesses were compared with the results of standard methods. Online and offline (62-83 µm) terahertz and SEM (66-75 µm) measurements delivered the best agreement for average coating thickness. In contrast, mechanical testing methods gave either too low or too high values for layer thickness, which were not comparable. Terahertz time-domain spectroscopy and imaging technology enable the first non-destructive quality control of acrylate-based textile coatings immediately following coating in the production line. Measurable variables are coating thicknesses and the detection of defects such as air inclusions.