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Abstract
The chelate oxides of bis(trimethylantimony) (Me3SbL1)2O (i = 1 or 2, L1-acetylacetonate, L2 - trifluoroacetylacetonate) and bis(triethylantimony) (Et3SbL1)2O have been obtained in 79–85% yields by a one-step oxidation of trialkylantimony withtertbutylhydroperoxide in the presence of β-diketones in benzene at 20 °C.
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