Abstract
In this present paper, using NiCO3⋅2Ni(OH)2⋅4H2O as raw material and small iron milling balls (ϕ=1.0–1.5mm) as the supply of Fe source, well-ordered ellipsoidal nickel ferrite particles were directly synthesized at low temperature of ≤100°C in 20h, without the need of calcination, via ultrasonic-assisted solid–liquid reaction ball milling technique. The results showed that ultrasonic wave assistance enables the intermediate product (Fe2Ni2(OH)8CO3⋅2H2O), produced using NiCO3⋅2Ni(OH)2⋅4H2O as raw material, to react with Fe more easily, by which NiFe2O4 is one-step synthesized. Finally, compared with conventional process, this milling technique is simple and environment friendly for obtained function ferrite nanopowders.
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