Abstract
3-Dichloromethylpyridine was synthesized by reaction of pyridine with the system MeOH-CCl4-iron catalyst [FeBr2, Fe3(CO)12, or iron(III) naphthenate]. Iron(II) bromide at a FeBr2-pyridine-CCl4-MeOH ratio of 1:100:200:200 showed the highest catalytic activity.
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