Abstract
An addition of benzaldehyde to an ethereal solution of tert-butyldimethylsilyldibromomethyllithium provided α-bromo-α-silyl ketone. Further treatment of the α-bromo-α-silyl ketone with butyllithium afforded enolate which provided β-hydroxy-α-silyl ketone upon treatment with aldehyde in ether. The enolate gave α,β-unsaturated ketone or monosilyl ether of 2-acyl-1,3-diol in THF instead of ether.
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