Abstract

BackgroundFraudulent milk adulteration is a dangerous practice in the dairy industry that is harmful to consumers since milk is one of the most consumed food products. Milk quality can be assessed by Fourier Transformed Infrared Spectroscopy (FTIR), a simple and fast method for obtaining its compositional information. The spectral data produced by this technique can be explored using machine learning methods, such as neural networks and decision trees, in order to create models that represent the characteristics of pure and adulterated milk samples.ResultsThousands of milk samples were collected, some of them were manually adulterated with five different substances and subjected to infrared spectroscopy. This technique produced spectral data from the milk samples composition, which were used for training different machine learning algorithms, such as deep and ensemble decision tree learners. The proposed method is used to predict the presence of adulterants in a binary classification problem and also the specific assessment of which of five adulterants was found through multiclass classification. In deep learning, we propose a Convolutional Neural Network architecture that needs no preprocessing on spectral data. Classifiers evaluated show promising results, with classification accuracies up to 98.76%, outperforming commonly used classical learning methods.ConclusionsThe proposed methodology uses machine learning techniques on milk spectral data. It is able to predict common adulterations that occur in the dairy industry. Both deep and ensemble tree learners were evaluated considering binary and multiclass classifications and the results were compared. The proposed neural network architecture is able to outperform the composition recognition made by the FTIR equipment and by commonly used methods in the dairy industry.

Highlights

  • Fraudulent milk adulteration is a dangerous practice in the dairy industry that is harmful to consumers since milk is one of the most consumed food products

  • In order to determine that the chosen techniques and machine learning models were adequate for our experiments, we conducted a test that compared the performance of methods that are simpler and more commonly used in the dairy industry: Logistic Regression, Linear Regression and Partial Least Squares (PLS) [6, 7]

  • All classifiers were evaluated with 3 pairs of training and test datasets randomly selected from our milk samples, identified by their proportion of training and test samples

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Summary

Introduction

Fraudulent milk adulteration is a dangerous practice in the dairy industry that is harmful to consumers since milk is one of the most consumed food products. Milk quality can be assessed by Fourier Transformed Infrared Spectroscopy (FTIR), a simple and fast method for obtaining its compositional information. Milk fraudulent adulteration consists of adding foreign substances to the milk. This is a common practice in Brazil and several countries worldwide [12], with the objective of increasing the product volume, disguising poor quality parameters and profiting with illegal actions [2, 7, 22]. Hydrogen peroxide and formaldehyde can preserve microbial count related to poor milk quality [9]

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