Abstract

Over the last years heat treatment concept of “quenching and partitioning” (Q&P) has reached popularity for its ability to precisely adjust material properties to desired values. Mostly, Q&P process are applied on tailor-made materials with high purities or prototype alloys. The research in hand presents the whole routine of how to investigate the potential of a commercial 0.54C-1.45Si-0.71Mn spring steel in terms of Q&P heat treatment from lab scale in dilatometer measurements to widely used inductive heat treatment on larger scale. In order to obtain the small process window for this material we were focusing on the interplay of the formed microstructure and the resulting mechanical properties in hardness measurements, compression tests as well as tensile tests. After full austenitizing, three different Q&P processing routes were applied. Microstructural analyses by optical microscopy, Scanning Electron Microscopy (SEM) and Electron Backscatter Diffraction (EBSD) exhibit a condition with 6.4% and 15% volume fraction of fine distributed retained austenite. Interestingly, the 15% of retained austenite developed during the partitioning heat treatment. Contradictory to our expectations, tensile and compression testing were showing that the 6.4% condition achieved improved mechanical properties compared to the 15% retained austenite condition. The remarkable conclusion is that not only volume fraction and fine distribution of retained austenite determines the potential of improving mechanical properties by Q&P in commercial alloys: also the process step when the retained austenite is developing as well as occurring parallel formation of carbides may strongly influence this potential.

Highlights

  • The heat treatment concept of quenching and partitioning (Q&P) offers a lot of potential for numerous fields of application

  • The short duration of the Q&P heat treatment is addressed to industrial needs

  • Q&P treatment microstructure was analyzed by Electron Backscatter Diffraction (EBSD)

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Summary

Introduction

The heat treatment concept of quenching and partitioning (Q&P) offers a lot of potential for numerous fields of application. Excellent properties of quenched and partitioned steels are based on the distinctive microstructure containing martensite and retained austenite, the latter of which was stabilized to room temperature by carbon diffusion from supersaturated martensite. Aim of the Q&P treatment is to induce formation of a fine-grained microstructure containing tempered martensite laths surrounded by small areas of stabilized retained austenite leading to good formability of the material [1,2,3,4]. The motivation of this study is to improve the conventional Q&T properties for a lower alloyed spring steel (reduced Cr content), with shorter processing times and without any molten salts or tempered oil baths In this way, the potential towards industrial application of the process should be underlined.

Materials and Methods
Micrographs
Dilatometric graph hardening of out
Results and Discussion aand
Microstructure
Mechanical
Mechanical Properties
SEM Analysis of Fracture Surfaces
Fracture
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