Abstract

Cobalt doped ZnO nanoparticles were synthesized by microwave irradiation technique for their structural and magnetic properties. Initially the samples were exhibit single phase standard ZnO wurtzite structure ( x ≤ 0.1) further Co concentration increase Co 3 O 4 phase was confirmed by X-ray diffraction analysis. The average crystallite sizes of cobalt doped ZnO particles were calculated by Debye-Scherrer formula and are nearly 25 nm. The hexagonal wurtzite structure of ZnO and destroyed cubical Co 3 O 4 were identified in the TEM images. The presence of metal oxide was confirmed by Fourier transform infrared spectral analysis result. The micro-Raman analysis confirmed the existence of Co 3 O 4 phase. Magnetization measurements performed by using vibrating sample magnetometer determine the paramagnetic behavior for the synthesized samples.

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