Abstract

The microstructure of as-grown TiN whisker-like crystals was examined using Lang X-ray topography, transmission electron microscopy (TEM) and also the Eshelby measurement of the twist of the crystal lattice. It was found that the as-grown TiN whisker-like crystals exhibit a very high degree of structural perfection. In a few cases the observed dislocations were deformation-type dislocations and occurred only in areas of brittle fracture of whiskers. In none of the tested as-grown whisker-like crystals axial dislocations were detected.

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