Numerical characterization of acid fracture wall etching morphology and experimental investigation on sensitivity factors in carbonate reservoirs

Abstract

Carbonate reservoirs are marked by their low porosity and permeability, naturally occurring fractures that develop in a stochastic fashion and exhibit significant heterogeneity. Deep acidification techniques are essential for the efficient development of such oil and gas reservoirs. The effective distance of acid etching (acid etch fracture length) and the fracture conductivity stand as the two most critical parameters for assessing the efficacy of acidizing. The primary objective of using this technique is to extend the effective distance of the acid etch and enhance the fracture conductivity. The "relay-style" full-length acid etched fracture testing method is employed, achieving an accurate match between the testing temperature, pressure, fracture length, and the actual acid fracturing conditions. It employs a large-scale rock plate acid etching experimental device, in conjunction with 3D laser scanning technology, and utilizes orthogonal experimental design methods to conduct detailed numerical characterization of the rock plate fracture surfaces before and after etching with various acid fluid types, acid injection amounts, and acid injection rates. It quantifies the change in the concentration of the residual acid fluid after the acid-rock reaction, calculating the etching volume of the acid fluid and the length of the acidizing fracture. The experimental results demonstrate that both the gelled acid and the clean diverting acid exhibit long acidification distances and strong inhomogeneous etching capabilities. The etch morphology of the clean diverting acid is dominated by pitting-type and stripe-like dissociation, exhibiting a wavy pattern. In contrast, the etch morphology of the gelled acid appears band-like and groove-like. As the acid injection amount increases, the etch length increases. Under on-site working conditions, etch lengths of 46.42 m and 41.63 m were recorded for 20% gelled acid and clean diverting acid, respectively, after 60 min acid injection time. The factors affecting the etch length sensitivity are in the following order: acid injection rate > acid type > etching time. The optimal acid fracturing parameters to achieve the maximum etch length are: The etch is performed at a pump rate of 600 mL/min for 90 min using gelled acid. Quantitative characterization of acid etch fracture morphology can optimize designing parameters of acid fracturing techniques, enhance the efficiency of their modification, and further enhance the development benefits of oil and gas carbonate rock reservoirs.