Abstract
The kinetics of the reactions of OO-diethyl S-hydrogen phosphorodithioate and O-ethyl S-hydrogen methylphosphonodithioate with p-nitrophenylketen dialkyl acetals in di-n-butyl ether as solvent are reported and discussed in terms of a mechanism which involves a highly reversible protonation (probably to an ion-pair) followed by nucleophilic attack by the phosphorus anion on the intermediate carbonium ion of the ion-pair.
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