Abstract
The 35Cl Nuclear Quadrupole Resonance spectra of two cyclic phosphorus-containing compounds, ((CH 3) 2PO 2SbCl 4) 2 and (Cl 2PO 2SbCl 4) 2, and five sulphur-containing compounds, (RSO 3SbCl 4) 2, which have been supposed to have similar structures, are reported. The NQR spectra support the hypothesis that the sulphur compounds have similar structures to the phosphorus compounds while showing that for (FSO 3SbCl 4) 2 the symmetry of the eight- membered ring is different from that of the other six compounds.
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