Abstract
Palladium nanoparticles with controlled size were synthesized within the pores of the mesoporous SBA-15 and SBA-16 silicas with grafted silicon hydride groups. Nitrogen adsorption-desorption method, X-ray diffraction and transmission electron microscopy (TEM) were used for characterization of palladium-containing composites. Results of material study clearly revealed that Pd nanoparticles prepared by this method were located inside the porous channels and were quite uniform in size (mostly 5–6 nm). The influence of metal content on the particles size and porous structure of supports was investigated.
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