Abstract
A novel dimerized Ni-dithiolene complex, ( n -Bu 4 N) 2 [Ni(dmit)( i -mnt)] 2 ( 1 ), was synthesized and characterized by X-ray structure analysis. In this complex two [Ni(dmit)( i -mnt)] units were mutually connected by two long axial Ni-S bonds. The single crystals of TTF, BEDT-TTF and EDT-TTF salts with [Ni(dmit)( i -mnt)] 2 2− were prepared by electrocrytallization and characterized by X-ray analyses. The Ni-S bonds of each dimer were also retained in these salts. Each salt exhibited semiconducting behavior.
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