Abstract
Vanadyl(2+) hydrogen phosphate hemihydrate (VOHPO 4 .0.5H 2 O, VHP) that had high crystallinity and showed a strong (001) peak in its X-ray diffractometry (XRD) pattern was synthesized via thermal treatment of a mixture of vanadyl(2+) acetylacetonate and triethyl phosphate at 200°C in organic solvents that contained a small amount of water. Scanning electron microscopy observations revealed that the product consisted of thin plates (2-4 μm wide and 20 μm. The present VHP sample was topotactically transformed to divanadyl(2+) pyrophosphate, which showed a strong (020) XRD peak, via thermal treatment in a nitrogen atmosphere at 500°C.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
