Abstract
An X-ray structural study of the trinuclear complex Fe 3(CO) 7[Pn 2PC 4(CF 3) 2 PPh 2 (I) has shown that the conversion of another trinuclear complex Fe 3(CO) 8[Ph 2PC 4(CF 3) 2]PPh 2 (II) to (I) involves intramolecular CO elimination, metalmetal bond formation and novel structural changes in a diphenylphosphide bridge.
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