Abstract
A novel bimetallic Cr3Yb3 coordination compound containing a 3d-4f heterometallic Cr2Yb3 cationic cluster has been synthesized and structurally characterized. The crystal structure was determined by X-ray analysis. Results denote that the complex consists of an original [Cr2IIIYb3III]3+ moiety with a trigonal-bipyramidal topology of the [Cr2Yb3(μ-OOCCH3)6(μ-OH)6(H2O)6]3+ core, an isolated [CrIII(CN)6]3− anion, and four molecular neutral 4,4′-bipyridene (Bipy) ligands, namely, [Cr2Yb3(μ-OOCCH3)6(μ-OH)6(H2O)6][Cr(CN)6] · 4Bipy · 13H2O.
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