Abstract
Abstract Pale brown single crystals of the title compound have been obtained by the reaction of Pb[N(SiMe3)2]2 with molybdenum pentachloride in ether solution as a result of a redox reaction. ClPb[N(SiMe3)2]3 crystallizes in the trigonal space group R3 with three formula units per unit cell. Lattice dimensions at -50 °C: a = b -1828.7(2), c = 854.5(1) pm. The compound forms monomeric molecules with bond lengths Pb-Cl = 247.9(4) pm and Pb - N = 213(2) pm.
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