Abstract

The determination of the mechanical properties of materials is predominantly undertaken using destructive approaches. Such approaches are based on well-established mathematical formulations where a physical property of the material is measured as a function of an input under controlled conditions provided by some machine, such as load–displacement curves in indentation tests and stress–strain plots in tensile testing. The main disadvantage of these methods is that they involve destruction of samples as they are usually tested to failure to determine the properties of interest. This means that large sample sizes are required to obtain statistical certainty, a condition that, depending on the material, may mean the process is both time consuming and expensive. In addition, for rapid prototyping and small-batch manufacturing of polymers, these techniques may be inappropriate either due to excessive cost or high polymer composition variability between batches. In this paper we discuss how the Euler–Bernoulli beam theory can be exploited for experimental, non-destructive assessment of the mechanical properties of three different 3D-printed materials: a plastic, an elastomer, and a hydrogel. We demonstrate applicability of the approach for materials, which vary by several orders of magnitude of Young’s moduli, by measuring the resonance frequencies of appended rectangular cantilevers using laser Doppler vibrometry. The results indicate that experimental determination of the resonance frequency can be used to accurately determine the exact elastic modulus of any given 3D-printed component. We compare the obtained results with those obtained by tensile testing for comparison and validation.

Highlights

  • Modelling (FDM), stereolithography (STL), or digital light processing (DLP), can produce materials with contrasting mechanical properties—from soft to hard plastics, alloys, hydrogels, and elastomers—that can be applied in several areas of scientific research [6,7,8,9,10]

  • For 3D-printed materials, the mechanical properties will be dependent on layer orientation and exposure time in addition to any post-curing and post-processing of parts, leading to high variability and meaning that large sample sizes are required for accuracy

  • We demonstrate the use of the Euler–Bernoulli beam theory to experimentally determine the elastic modulus of 3D-printed materials, including plastics, elastomers, and hydrogels, which range from GPa to a few kPa

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Summary

Introduction

Modelling (FDM), stereolithography (STL), or digital light processing (DLP), can produce materials with contrasting mechanical properties—from soft to hard plastics, alloys, hydrogels, and elastomers—that can be applied in several areas of scientific research [6,7,8,9,10]. Mathematical models exist in the literature to allow mechanical properties of these new materials to be estimated as a function of the matrix and filler densities and concentrations [11], but they still require individual testing of the different components for accurate results These theoretical formulations are based on assumptions regarding the homogeneity of any filler distribution, uniformity of particle size, and isotropic properties. For 3D-printed materials, the mechanical properties will be dependent on layer orientation and exposure time in addition to any post-curing and post-processing of parts, leading to high variability and meaning that large sample sizes are required for accuracy. This limitation results in longer exposure times, resulting in inhomogeneous crosslinking densities within the material

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