Abstract
[1696-17-9] C11H15NO (MW 177.246) InChI = 1S/C11H15NO/c1-3-12(4-2)11(13)10-8-6-5-7-9-10/h5-9H,3-4H2,1-2H3 InChIKey = JLNGEXDJAQASHD-UHFFFAOYSA-N Physical Data: mp 28–32 °C; bp 146–150 °C/15 mmHg;fp>100 °C. Solubility: soluble in most of the organic solvents. Form Supplied in: colorless oil. Analysis of Reagent Purity: NMR, IR, mass spectrometry. Handling, Storage, and Precautions: the compound should be handled with protective gloves and eyewear in a ventilated area. Preparative Methods: the title product can be obtained by reaction between benzoyl chloride and diethylamine in the presence of triethylamine in dichloromethane at room temperature1 or by a Cannizzaro reaction between benzaldehyde and lithium diethylamide in THF at 0 °C.2 Purification: flash chromatography using 40% EtOAc in hexanes.
Published Version
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